RheoCheck: Test Results
Below you can find the description of the test results produced by RheoCheck software



 

MI: Initial Torque 
This calculation returns the Maximum Torque recorded at Test Start.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')


ML: Minimum Torque 
This calculation returns the minimum torque value measured during the test;

The calculation provides useful information regarding the viscosity of the green compound at test temperature.
For example, this information may be useful for:
- the correct evaluation of the force needed for injection moulding (depending from the shape of the mould and the size of the injection channels)
- the setting of temperature and force for extrusion process.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')




tML: Time at Minimum Torque 
This calculation returns the time, from the start of the test, when the ML point is reached (in the case of maintenance of the ML value over a period of time, it represents the termination point of the interval)

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')


MH: Maximum Torque 
This calculation returns the maximum torque value measured during the established test time.

Depending from the product under test, from the test time selected and from the test temperature, the curve may have reached a plateau value or not
This calculation is an indication of the mechanical characteristics of the cured compound and has positive correlation with other mechanical properties like hardness and tensile stress at set strain.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')


tMH: Time at Maximum Torque 
This calculation returns the time, from the start of the test, when the MH point is reached (in the case of maintenance of the MH value over a period of time, it represents the starting point of the interval)

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')




ts_x: Scorch Time 
The Scorch time tsx is the time required for the torque to increase by x units from ML. The typical value of x for an MD Rheometer is 1 dN•m.

The scorch time (time to incipient cure) tsx is a measure of the processing safety of the compound.
For injection moulding, it provides a relative indication of the maximum available time for the complete filling of the cavities.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')


t'_x: time to set percentage of curing  
The time to a percentage of full cure from minimum torque t’_x is the time taken for the torque to reach: ML + x*(MH-ML)/100
Frequently used values of t’_x are:
- t’_10: is a measure of the early stages of cure
- t’_50: provides the slope of the curve is greatest at this point.
- t’_90: is often used as an indicator of optimum press cure

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Percentage of Curing desired.
Reference Curve (0=S*,1=S')


M_x: torque at set percentage of curing  
Torque at a percentage of full cure from minimum torque M_x is the torque value at: ML + x*(MH-ML)/100

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Percentage of Curing desired.
Reference Curve (0=S*,1=S')




Tanƌ@ML: Tangent of ƌ at Minimum Torque  
This calculation returns the reading of the Tanƌ curve when S' curve reaches ML.
The calculation is an expression of visco-elastic properties of the uncured sample.

UNIT: num


Tanƌ@MH: Tangent of ƌ at Maximum Torque  
This calculation returns the reading of the Tanƌ curve when S' curve reaches MH.
The calculation is an expression of visco-elastic properties of the cured sample.

UNIT: num


S"@ML: Viscous curve at Minimum Torque  
This calculation returns the reading of the S" curve when S' curve reaches ML.
The calculation is an expression of viscous properties of the uncured sample.

UNIT: dN*m or Lbf*In




S"@MH: Viscous curve at Maximum Torque  
This calculation returns the reading of the S" curve when S' curve reaches MH.
The calculation is an expression of viscous properties of the cured sample.

UNIT: dN*m or Lbf*In


tR_x: Time for Reversion of x dN*m  
This calculation returns the time from test start, when a torque reduction of x dN*m from MH is detected.
The calculation is an expression of the degradation of the sample at the testing conditions.

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Torque decay compared to MH
Reference Curve (0=S*,1=S')


Rev_t: Reversion at set Time 
This calculation returns the torque reduction from MH at the set test time.
The calculation is an expression of the degradation of the sample at the testing conditions.

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Test time
Reference Curve (0=S*,1=S')




MCR: Maximum Curing Rate 
This calculation returns the maximum torque increase value in the time unit measured during the test (corresponds to flexure point of the increasing line of the elastic curve S')

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m/sec


TMCR: Time at Maximum Curing Rate 
This calculation returns the time from test start at Maximum Cure Rate

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds


CRI: Cure Rate Index 
This calculation returns 100/(t'90 - ts2).
The cure rate index is the average slope of the rising curve.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: 1/min




MH-ML: Torque Increase 
This calculation returns the torque increase between the minimum value (ML) and the maximum one (MH)

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m, Lbf*in



Gibitre Instruments
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Below you can find the description of the test results produced by RheoCheck software
Campi di applicazione  >  Prove su pneumatici  >  Rheocheck MD - Drive
RheoCheck: Test Results
rheometer formulas: Software Rheometro: Software calculation formulas. Delta tnagent.

Below you can find the description of the test results produced by RheoCheck software

Applications

MI: Initial Torque 

This calculation returns the Maximum Torque recorded at Test Start.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of MI (Initial Torque) value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of MI (Initial Torque) value calculation.

ML: Minimum Torque 

This calculation returns the minimum torque value measured during the test;

The calculation provides useful information regarding the viscosity of the green compound at test temperature.
For example, this information may be useful for:
- the correct evaluation of the force needed for injection moulding (depending from the shape of the mould and the size of the injection channels)
- the setting of temperature and force for extrusion process.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of ML (Minimum Torque) value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of ML (Minimum Torque) value calculation.

tML: Time at Minimum Torque 

This calculation returns the time, from the start of the test, when the ML point is reached (in the case of maintenance of the ML value over a period of time, it represents the termination point of the interval)

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of ML (Minimum Torque) value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of ML (Minimum Torque) value calculation.
 

MH: Maximum Torque 

This calculation returns the maximum torque value measured during the established test time.

Depending from the product under test, from the test time selected and from the test temperature, the curve may have reached a plateau value or not
This calculation is an indication of the mechanical characteristics of the cured compound and has positive correlation with other mechanical properties like hardness and tensile stress at set strain.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of MH (Max Torque) value.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of MH (Max Torque) value.

tMH: Time at Maximum Torque 

This calculation returns the time, from the start of the test, when the MH point is reached (in the case of maintenance of the MH value over a period of time, it represents the starting point of the interval)

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of MH (Max Torque) value.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of MH (Max Torque) value.

ts_x: Scorch Time 

The Scorch time tsx is the time required for the torque to increase by x units from ML. The typical value of x for an MD Rheometer is 1 dN•m.

The scorch time (time to incipient cure) tsx is a measure of the processing safety of the compound.
For injection moulding, it provides a relative indication of the maximum available time for the complete filling of the cavities.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of calculation of Ts_X value (time per scorch of x points).
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of calculation of Ts_X value (time per scorch of x points).

t'_x: time to set percentage of curing  

The time to a percentage of full cure from minimum torque t’_x is the time taken for the torque to reach: ML + x*(MH-ML)/100
Frequently used values of t’_x are:
- t’_10: is a measure of the early stages of cure
- t’_50: provides the slope of the curve is greatest at this point.
- t’_90: is often used as an indicator of optimum press cure

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Percentage of Curing desired.
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of t':XX (time to reach the percentage XX of cross-linking).
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of t':XX (time to reach the percentage XX of cross-linking).

M_x: torque at set percentage of curing  

Torque at a percentage of full cure from minimum torque M_x is the torque value at: ML + x*(MH-ML)/100

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Percentage of Curing desired.
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of t':XX (time to reach the percentage XX of cross-linking).
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of t':XX (time to reach the percentage XX of cross-linking).

Tanƌ@ML: Tangent of ƌ at Minimum Torque  

This calculation returns the reading of the Tanƌ curve when S' curve reaches ML.
The calculation is an expression of visco-elastic properties of the uncured sample.

UNIT: num

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of Tang_Delta@ML (Tangent of Delta at the minimum torque point).
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of Tang_Delta@ML (Tangent of Delta at the minimum torque point).

Tanƌ@MH: Tangent of ƌ at Maximum Torque  

This calculation returns the reading of the Tanƌ curve when S' curve reaches MH.
The calculation is an expression of visco-elastic properties of the cured sample.

UNIT: num

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of Tang_Delta@MH (Tangent of Delta at the point of maximum torque).
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of Tang_Delta@MH (Tangent of Delta at the point of maximum torque).

S"@ML: Viscous curve at Minimum Torque  

This calculation returns the reading of the S" curve when S' curve reaches ML.
The calculation is an expression of viscous properties of the uncured sample.

UNIT: dN*m or Lbf*In

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of S
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of the calculation of the value of S"@ML.

S"@MH: Viscous curve at Maximum Torque  

This calculation returns the reading of the S" curve when S' curve reaches MH.
The calculation is an expression of viscous properties of the cured sample.

UNIT: dN*m or Lbf*In

rheometer formulas: What is required by the standards and something more
What is required by the standards and something more

tR_x: Time for Reversion of x dN*m  

This calculation returns the time from test start, when a torque reduction of x dN*m from MH is detected.
The calculation is an expression of the degradation of the sample at the testing conditions.

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

CALCULATION PARAMETERS:
Torque decay compared to MH
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of tr (reversion time) value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of tr (reversion time) value calculation.

Rev_t: Reversion at set Time 

This calculation returns the torque reduction from MH at the set test time.
The calculation is an expression of the degradation of the sample at the testing conditions.

UNIT: dN*m or Lbf*In

CALCULATION PARAMETERS:
Test time
Reference Curve (0=S*,1=S')

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of Reversion value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of Reversion value calculation.

MCR: Maximum Curing Rate 

This calculation returns the maximum torque increase value in the time unit measured during the test (corresponds to flexure point of the increasing line of the elastic curve S')

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m/sec

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of MCR (Max Cure Rate) value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of MCR (Max Cure Rate) value calculation.

TMCR: Time at Maximum Curing Rate 

This calculation returns the time from test start at Maximum Cure Rate

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: mm:cc (minutes, minutes/100) or mm:ss (minutes, seconds) or Seconds

rheometer formulas: Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of MCR (Max Cure Rate) value calculation.
Gibitre software. Formulas for calculating results. Rheo-Check software. Graphical explanation of MCR (Max Cure Rate) value calculation.

CRI: Cure Rate Index 

This calculation returns 100/(t'90 - ts2).
The cure rate index is the average slope of the rising curve.

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: 1/min

MH-ML: Torque Increase 

This calculation returns the torque increase between the minimum value (ML) and the maximum one (MH)

REFERENCE STANDARD: ISO 6502-1, ISO 6502-3

UNIT: dN*m, Lbf*in

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MooneyCheck: Test Results
Vedi anche: Mooney viscometer: software calculation formulas: scorch time.
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